p-Chlorothiophenol → HCID 24953920, compound

HRID 1946972Notes

Reaction equation

HRID 1946972 reaction equation
Cl[CH2:2][C:3]1[N:4]=[CH:5][N:6](C(C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)[C:7]=1[CH3:8].[Cl:28][C:29]1[CH:34]=[CH:33][C:32]([SH:35])=[CH:31][CH:30]=1>>[Cl:28][C:29]1[CH:34]=[CH:33][C:32]([S:35][CH2:2][C:3]2[N:4]=[CH:5][NH:6][C:7]=2[CH3:8])=[CH:31][CH:30]=1

Participants

3

Reactant 2

HCID 7815p-ChlorothiophenolHCID 110469654-(Chloromethyl)-5-methyl-1-trityl-1H-imidazole

Product 1

HCID 24953920HCID 24953920, compound

Procedure

The title compound was prepared in analogy to example 42 using 4-chloromethyl-5-methyl-1-trityl-1H-imidazole (CAS106147-85-7) for the alkylation of 4-chlorobenzenethiol.

Sources & evidence

ORD record
ord-c617384109e34d5bb23596f0e1c1e98b
Source dataset
uspto-grants-2013_03
Patent number
US08399463B2

Reaction notes

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