Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1947130Generated: November 2, 2026

Ethanol → HCID 66893306, compound

https://huagongshe.com/reaction/1947130

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantHydrogen chloride-ethyl acetateHCID 21866389—
ReactantHCID 44226452HCID 44226452—
SolventEthyl AcetateHCID 8857—
ProductHCID 66893306HCID 6689330645%

Reaction Steps

To a solution of the compound of Example 79 (150 mg, 0.290 mmol) in ethyl acetate (4 mL)/ethanol (6 mL) was added 4N hydrogen chloride ethyl acetate solution (80.0 μL). The precipitate was collected by filtration, washed with ethyl acetate, and dried under reduced pressure to give the title compound (72 mg, 45%) as a white powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08399449B2
Source datasetuspto-grants-2013_03
ORD IDord-e0bf4d6d3bf34a1e9779571f223d6dac
Source noteuspto-grants-2013_03