HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 66893306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 44226452 | HCID 44226452 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 66893306 | HCID 66893306 | 45% |
Reaction Steps
To a solution of the compound of Example 79 (150 mg, 0.290 mmol) in ethyl acetate (4 mL)/ethanol (6 mL) was added 4N hydrogen chloride ethyl acetate solution (80.0 μL). The precipitate was collected by filtration, washed with ethyl acetate, and dried under reduced pressure to give the title compound (72 mg, 45%) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399449B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-e0bf4d6d3bf34a1e9779571f223d6dac |
| Source note | uspto-grants-2013_03 |