huagongshe.com
HRID1947260

反应详情

EQUATION

反应方程式

HRID 1947260 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1ccc(I)cc1
HCID96657

Benzaldehyde, 4-iodo-

C7H5IO

结构：COC(=O)CCCN1C(=O)N=C(NC2CCCCC2)C12CCNCC2.Cl.Cl
HCID178500498

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)CCCN1C(=O)N=C(NC2CCCCC2)C12CCN(Cc1ccc(I)cc1)CC2
HCID178500496

未命名化合物

PROCEDURE

实验过程

Reductive amination using methyl 4-[4-(cyclohexylamino)-2-oxo-1,3,8-triazaspiro[4.5]dec-3-en-1-yl]butanoate dihydrochloride and 4-iodo-benzaldehyde using a similar procedure as described in the preparation of intermediate I.1.d.1. LRMS (M+1)=567.5.

WORKUP

后处理

  1. customas described in the preparation of intermediate I.1.d.1