Methanesulfonyl chloride → HCID 68770949, compound

Participants

Reaction Steps

To a solution of 1-[6-(thiazolo[4,5-b]pyridin-2-yloxy)-benzofuran-2-ylmethyl]-pyrrolidin-3-ylamine (126 mg, 0.313 mmol) in DMF (2 mL) was added DIEA (125 μL, 0.938 mmol) followed by MsCl (72 μL, 0.938 mmol) and the resulting solution was stirred (rt, 1 h). The reaction mixture was filtered (Celite®) and concentrated in vacuo.

Provenance & Evidence