Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Bromobenzyl bromide → 1-Bromo-4-((methylsulfonyl)methyl)benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Bromobenzyl bromide | HCID 68527 | — |
| 반응물 | HCID 178504973 | HCID 178504973 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-Bromo-4-((methylsulfonyl)methyl)benzene | HCID 2761415 | — |
반응 단계
p-Bromobenzyl bromide (500 mg, 2 mmol) was refluxed with MeSO2Na (306 mg, 3 mmol) in Ethanol for 1 hour. The reaction was cooled, concentrated and purified by flash column (50% acetone/hexanes) to give the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08399485B2 |
| 출처 데이터셋 | uspto-grants-2013_03 |
| ORD ID | ord-82384adefcaf4174bf938a044b1f39c4 |
| 출처 메모 | uspto-grants-2013_03 |