HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dipropan-2-yl(3-nitrophenyl)phosphonate → Dipropan-2-yl(3-aminophenyl)phosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dipropan-2-yl(3-nitrophenyl)phosphonate | HCID 54035471 | — |
| Reactant | Dipropan-2-yl(4-aminophenyl)phosphonate | HCID 86653993 | — |
| Product | Dipropan-2-yl(3-aminophenyl)phosphonate | HCID 13649474 | 45% |
Reaction Steps
Prepared according to the procedure described for dipropan-2-yl(4-aminophenyl)phosphonate using dipropan-2-yl(3-nitrophenyl)phosphonate. Yield: 45%. 1H-NMR (DMSO-d6, 400 MHz): δ=1.15 (d, J=6.4 Hz, 6H), 1.24 (d, J=6.4 Hz, 6H), 4.45-4.50 (m, 2H), 5.35 (s, br, 2H), 6.70-6.77 (m, 2H), 6.58 (d, J=8.0 Hz, 1H), 7.10-7.25 (m, 1H). MS: m/z 257.97 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399433B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-0591b0b752644f64b1405f8843160ee7 |
| Source note | uspto-grants-2013_03 |