HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluoro-5-methoxy-4-nitrobenzoic acid → (3-Fluoro-5-methoxy-4-nitrophenyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluoro-5-methoxy-4-nitrobenzoic acid | HCID 57955522 | — |
| Reactant | 2-Fluoro-5-methoxy-4-nitrobenzoic acid | HCID 57955614 | — |
| Product | (3-Fluoro-5-methoxy-4-nitrophenyl)methanol | HCID 67256643 | — |
Reaction Steps
The title compound was prepared using the procedure from Compound 130E (2-fluoro-5-methoxy-4-nitrobenzoic acid) with 3-fluoro-5-methoxy-4-nitrobenzoic acid (Compound 146E). 1H NMR (CDCl3, 400 MHz): δ=3.95 (s, 3H), 4.76 (s, 2H), 6.81-6.86 (m, 1H), 6.88 (s, 1H). MS (ES+): m/z 202.05 [MH+] (TOF, polar).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399433B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-433bdaa29b7a46fc919069dc14babeb4 |
| Source note | uspto-grants-2013_03 |