HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Aminophenyl)(4-methylpiperazin-1-yl)methanone → HCID 58292912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Aminophenyl)(4-methylpiperazin-1-yl)methanone | HCID 550840 | — |
| Reactant | Diethyl (4-{[4-chloro-5-(trifluoromethyl) pyrimidin-2-yl]amino}-3-methoxybenzyl)phosphonate | HCID 86654002 | — |
| Product | HCID 58292912 | HCID 58292912 | — |
Reaction Steps
The title product was prepared according to the procedure for Example 102 using diethyl(4-{[4-chloro-5-(trifluoromethyl)pyrimidin-2-yl]amino}-3-methoxybenzyl)phosphonate and the commercially available (2-aminophenyl)-(4-methylpiperazin-1-yl)-methanone. MS (ES+): m/z 637.40 (100) [MH+]; HPLC: tR=0.69 min (UPLC, purity).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399433B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-60bbafa81f2f40d18fd9a54f659ce196 |
| Source note | uspto-grants-2013_03 |