Methanesulfonyl chloride → HCID 69345356, compound

Participants

Reaction Steps

According to Scheme 26 Step 2: The title compound was prepared from 1-(6-methoxypyridin-3-yl)cyclohexanol (1 eq, 1.21 mmol, 0.25 g) and methanesulfonyl chloride (4 eq, 4.82 mmol, 0.37 mL) according to the procedure described for Example 4 Step 1. The crude residue was purified by chromatography over silicagel (AIT Flashsmart prepacked column 10 g SiO2, AcOEt/pentane 30/10 to pure AcOEt), yielding the title compound (0.76 mmol, 0.14 g, 63%) as a colorless oil.

Provenance & Evidence