(Naphthalen-2-yl)boronic acid → HCID 21923471, compound

HRID 1948803Notes

Reaction equation

HRID 1948803 reaction equation
C1([C:7]2[N:12]=[C:11]([CH:13]=[O:14])[CH:10]=[CH:9][CH:8]=2)C=CC=CC=1.[CH:15]1[C:24]2[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=2)[CH:18]=[CH:17][C:16]=1B(O)O>>[CH:20]1[C:19]2[C:24](=[CH:15][C:16]([C:10]3[C:11]([CH:13]=[O:14])=[N:12][CH:7]=[CH:8][CH:9]=3)=[CH:17][CH:18]=2)[CH:23]=[CH:22][CH:21]=1

Participants

3

Reactant 2

HCID 2734375(Naphthalen-2-yl)boronic acidHCID 135224166-Phenylpyridine-2-carbaldehyde

Product 1

HCID 21923471HCID 21923471, compound

Procedure

Precursor (D) was prepared following the same procedure as that used to prepare precursor (A) except that 206 mg (1.2 mmol) of 2-naphthylboronic acid were used as reagent. 190 mg of precursor (D) were obtained as colourless oil with a yield of 82%.

Workup

  1. customPrecursor (D) was prepared

Sources & evidence

ORD record
ord-520819d0b66049849f5cbba9f1f61182
Source dataset
uspto-grants-2013_03
Patent number
US08399582B2

Reaction notes

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