8-Quinolineboronic acid → HCID 59378677, compound

HRID 1948804Notes

Reaction equation

HRID 1948804 reaction equation
[C:1]1([C:7]2[N:12]=[C:11]([CH:13]=[O:14])[CH:10]=[CH:9][CH:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[N:15]1C2C(=CC=CC=2B(O)O)[CH:18]=[CH:17][CH:16]=1>>[N:15]1[C:2]2[C:3](=[CH:4][CH:5]=[CH:6][C:1]=2[C:7]2[N:12]=[C:11]([CH:13]=[O:14])[CH:10]=[CH:9][CH:8]=2)[CH:18]=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 27343808-Quinolineboronic acidHCID 135224166-Phenylpyridine-2-carbaldehyde

Product 1

HCID 59378677HCID 59378677, compound

Procedure

Precursor (F) was prepared following the same procedure as that used to prepare precursor (A) except that 216 mg (1.2 mmol) of 8-quinolineboronic acid were used as reagent. 232 mg of precursor (F) were obtained as pale yellow solid with a yield of 99%.

Workup

  1. customPrecursor (F) was prepared

Sources & evidence

ORD record
ord-e8624d47bd704b199781402a327016a1
Source dataset
uspto-grants-2013_03
Patent number
US08399582B2

Reaction notes

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