2-Acetylpyridine → HCID 68607176, compound

HRID 1948807Notes

Reaction equation

HRID 1948807 reaction equation
[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][N:5]=1)(=O)[CH3:2].[NH2:10][C:11]1[CH:16]=[C:15]([N+:17]([O-:19])=[O:18])[CH:14]=[CH:13][C:12]=1[OH:20]>>[N:5]1[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=1[CH2:1][CH2:2][N:10]=[C:11]1[CH:16]=[C:15]([N+:17]([O-:19])=[O:18])[CH:14]=[CH:13][CH:12]1[OH:20]

Participants

3

Reactant 2

HCID 142862-AcetylpyridineHCID 36133892-Amino-4-Nitrophenol

Product 1

HCID 68607176HCID 68607176, compoundYield 30%

Procedure

Ligand L28 was prepared following the same procedure as that used to prepare ligand L27 except that 300 μL (2 mmol) of 2-acetylpyridine were used as reagent 1 and 321 mg (2 mmol) of 2-amino-4-nitrophenol as reagent 2. 156 mg of ligand L28 were obtained as dark yellow solid with a yield of 30%.

Workup

  1. customwere obtained as dark yellow solid with a yield of 30%

Sources & evidence

ORD record
ord-c4bd39237f4b4369b2603a6a2ec75625
Source dataset
uspto-grants-2013_03
Patent number
US08399582B2

Reaction notes

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