HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indole → HCID 45136983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indole | HCID 798 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 68650776 | HCID 68650776 | — |
| Product | HCID 45136983 | HCID 45136983 | — |
Reaction Steps
The title compound was prepared in a manner analogous to Example 70 except the starting indole is 5,7-diBOC-2,10-dibromo-6-(3-bromopropoxy)indolo[2,3-b]carbazole and the reagent is morpholine. 1H-NMR (400 MHz, DMSO-d6) δ ppm 11.28 (s, 2 H), 8.67 (s, 1 H), 8.28 (d, J=2.0 Hz, 2H), 7.51-7.40 (m, 4 H), 4.30 (t, J=6.6 Hz, 2 H), 3.56 (t, J=4.6 Hz, 4 H), 2.52 (t, J=7.2 Hz, 2 H), 2.44-2.32 (m, 4 H), 2.11-2.00 (m, 2 H); MS (ESI) m/z 556.0 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399502B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-2fe2bca81e8645b2ab800039d8653300 |
| Source note | uspto-grants-2013_03 |