m-Chlorophenylhydrazine hydrochloride → HCID 58277426, compound

HRID 1949211Notes

Reaction equation

HRID 1949211 reaction equation
Cl.ClC1C=C(NN)C=CC=1.[Cl:11][C:12]1[CH:13]=[C:14]([N:19]2[C:23]([C:24]3[CH:29]=[C:28]([F:30])[CH:27]=[C:26]([Cl:31])[CH:25]=3)=[CH:22][C:21]([C:32]([O:34][CH2:35][CH3:36])=[O:33])=[N:20]2)[CH:15]=[CH:16][C:17]=1F>>[Cl:31][C:26]1[CH:25]=[C:24]([C:23]2[N:19]([C:14]3[CH:15]=[CH:16][CH:17]=[C:12]([Cl:11])[CH:13]=3)[N:20]=[C:21]([C:32]([O:34][CH2:35][CH3:36])=[O:33])[CH:22]=2)[CH:29]=[C:28]([F:30])[CH:27]=1

Participants

3

Reactant 2

HCID 75331m-Chlorophenylhydrazine hydrochlorideHCID 58277311HCID 58277311, compound

Product 1

HCID 58277426HCID 58277426, compound

Procedure

The preparation of the title compound takes place starting from the compound of Example 1A and 3-chlorophenylhydrazine hydrochloride in analogy to the synthesis of the compound of Example 21A. 5.82 g of the title compound are obtained.

Sources & evidence

ORD record
ord-1fdf12ee23ee4593b53621517bf10de6
Source dataset
uspto-grants-2013_03
Patent number
US08399682B2

Reaction notes

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