3-Methoxyphenylhydrazine hydrochloride → HCID 58277408, compound

HRID 1949212Notes

Reaction equation

HRID 1949212 reaction equation
Cl.[CH3:2][O:3][C:4]1[CH:5]=[C:6]([NH:10][NH2:11])[CH:7]=[CH:8][CH:9]=1.ClC1C=C(N2[C:24]([C:25]3[CH:30]=[C:29]([F:31])[CH:28]=[C:27](Cl)[CH:26]=3)=[CH:23][C:22]([C:33]([O:35][CH2:36][CH3:37])=[O:34])=N2)C=CC=1F>>[F:31][C:29]1[CH:30]=[C:25]([C:24]2[N:10]([C:6]3[CH:7]=[CH:8][CH:9]=[C:4]([O:3][CH3:2])[CH:5]=3)[N:11]=[C:22]([C:33]([O:35][CH2:36][CH3:37])=[O:34])[CH:23]=2)[CH:26]=[CH:27][CH:28]=1

Participants

3

Reactant 2

HCID 27239403-Methoxyphenylhydrazine hydrochlorideHCID 58277311HCID 58277311, compound

Product 1

HCID 58277408HCID 58277408, compound

Procedure

The preparation of the title compound takes place starting from the compound of Example 8A and 3-methoxyphenylhydrazine hydrochloride in analogy to the synthesis of the compound of Example 21A. 30.4 g (62% of theory) of the title compound are obtained.

Sources & evidence

ORD record
ord-54495103fb214900bfb24bed940b5073
Source dataset
uspto-grants-2013_03
Patent number
US08399682B2

Reaction notes

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