m-Chlorophenylhydrazine hydrochloride → HCID 58277303, compound

HRID 1949218Notes

Reaction equation

HRID 1949218 reaction equation
Cl.Cl[C:3]1C=C(NN)C=CC=1.[Cl:11][C:12]1[CH:13]=[C:14]([N:19]2[C:23]([C:24]3[CH:29]=[C:28]([F:30])[CH:27]=[C:26](Cl)[CH:25]=3)=[CH:22][C:21]([C:32]([O:34][CH2:35][CH3:36])=[O:33])=[N:20]2)[CH:15]=[CH:16][C:17]=1F>>[Cl:11][C:12]1[CH:13]=[C:14]([N:19]2[C:23]([C:24]3[CH:25]=[C:26]([CH3:3])[CH:27]=[C:28]([F:30])[CH:29]=3)=[CH:22][C:21]([C:32]([O:34][CH2:35][CH3:36])=[O:33])=[N:20]2)[CH:15]=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 75331m-Chlorophenylhydrazine hydrochlorideHCID 58277311HCID 58277311, compound

Product 1

HCID 58277303HCID 58277303, compound

Procedure

The preparation of the title compound takes place starting from the compound of Example 20A and 3-chlorophenylhydrazine hydrochloride in analogy to the synthesis of the compound of Example 21A. 1.75 g of the title compound are obtained.

Sources & evidence

ORD record
ord-d3720f2fe0284853bb38c7992b2a7f76
Source dataset
uspto-grants-2013_03
Patent number
US08399682B2

Reaction notes

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