HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58277360, compound → HCID 58277269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58277360 | HCID 58277360 | — |
| Reactant | HCID 58277365 | HCID 58277365 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 58277269 | HCID 58277269 | — |
Reaction Steps
The preparation of the title compound takes place starting from the compound of Example 97A in analogy to the synthesis of the compound of Example 23 with the addition of 0.1% formic acid in the preparative HPLC. 60 mg (51% of theory) of the title compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399682B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-6e8d5a9681094fe8b17b84924db455df |
| Source note | uspto-grants-2013_03 |