HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 67153377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 58277334 | HCID 58277334 | — |
| Reactant | HCID 67153505 | HCID 67153505 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67153377 | HCID 67153377 | — |
Reaction Steps
The preparation of the title compound takes place starting from the compound of Example 120A and 1-methylpiperazine without the addition of tetrahydrofuran in analogy to the synthesis of the compound of Example 29. 45 mg (38% of theory) of the title compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399682B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-3a7e33ec9e714a189f5dc08839a6edb7 |
| Source note | uspto-grants-2013_03 |