HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-bromo-N-(2-chlorophenyl)-N-methyl-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamide → HCID 57900118, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-bromo-N-(2-chlorophenyl)-N-methyl-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamide | HCID 44242427 | — |
| Reactant | N-Boc-N-methyl-ethylenediamine (tert-butyl 2-aminoethyl(methyl)carbamate) | HCID 86634841 | — |
| Product | HCID 57900118 | HCID 57900118 | — |
Reaction Steps
Following the procedure of Example 13 and General Procedure C, 8-bromo-N-(2-chlorophenyl)-N-methyl-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamide 150 and N-Boc-N-methyl-ethylenediamine (tert-butyl 2-aminoethyl(methyl)carbamate) were reacted to give 139. MS: (ESI+) 470.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399690B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-59399c6323b248e6ba5728f3a21c6528 |
| Source note | uspto-grants-2013_03 |