HRID1949777

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID674

Dimethylamine

C2H7N

结构：O=C(O)c1ccc(N(CCO)C(=O)c2cc3c(s2)-c2ccccc2OCC3)c(Cl)c1

HCID57900330

3-Chloro-4-[[(4,5-dihydrothieno[3,2-d][1]benzoxepin-2-yl)carbonyl](2-hydroxyethyl)amino]benzoic acid

C22H18ClNO5S

PRODUCTS

生成物

结构：CN(C)C(=O)c1ccc(N(CCO)C(=O)c2cc3c(s2)-c2ccccc2OCC3)c(Cl)c1

HCID57900423

未命名化合物

收率 50%

PROCEDURE

实验过程

Following the procedure of Example 91, 3-chloro-4-(N-(2-hydroxyethyl)-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamido)benzoic acid and dimethylamine were reacted to give 220 (yield 50%). MS: (ESI+) 471.1

WORKUP

后处理

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