HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroaniline → HCID 86634852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroaniline | HCID 7240 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 86634853 | HCID 86634853 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86634852 | HCID 86634852 | — |
Reaction Steps
Reaction of 2-chloroaniline with 9-bromo-4,5-dihydro-6-oxa-1-thia-benzo[e]azulene-2-carbonyl chloride (prepared from the corresponding carboxylic acid using oxalyl chloride with catalytic N,N-dimethylformamide) yielded 9-bromo-4,5-dihydro-6-oxa-1-thia-benzo[e]azulene-2-carboxylic acid (2-chloro-phenyl)-amide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399690B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-d0e5544c91b040bbab519e638beaa68a |
| Source note | uspto-grants-2013_03 |