HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutyramide → [1-Dimethylamino-meth-(e)-ylidene]-isobutyramide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutyramide | HCID 68424 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Product | [1-Dimethylamino-meth-(e)-ylidene]-isobutyramide | HCID 87184356 | — |
Reaction Steps
Following the procedure for 449, Step 3, isobutyramide was reacted with DMF-DMA to afford the title compound as a yellow oil. 1H NMR (CDCl3): 8.39 (1 H, s), 3.10 (3 H, m), 3.07 (3 H, d, J=0.67 Hz), 2.68-2.56 (1 H, m), 1.17 (3 H, s), 1.18-1.11 (3 H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399690B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-d900d8bf1148473f9d079cb147a32855 |
| Source note | uspto-grants-2013_03 |