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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1950052Erstellt: 25. Oktober 2026

1-Bromo-4-fluoro-2-nitrobenzene → HCID 23087411, Verbindung

https://huagongshe.com/reaction/1950052

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-Bromo-4-fluoro-2-nitrobenzeneHCID 2773383—
Edukt6-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonateHCID 15330256—
EduktTributyl(4-fluoro-2-nitrophenyl)tinHCID 23087155—
ProduktHCID 23087411HCID 23087411—

Reaktionsschritte

Synthesized from 1-bromo-4-fluoro-2-nitrobenzene according to an analogous synthetic method to Preparation Example 76, tributyl(4-fluoro-2-nitrophenyl)tin (7.1 g) and 6-methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate (2.2 g) were used according to an analogous synthetic method to Preparation Example 77 to provide 3-(4-fluoro-2-nitrophenyl)-7-methoxy-1,2-dihydronaphthalene (1.4 g). The total amount of this compound was used according to an analogous synthetic method to Example 30 to provide the title compound (1.1 g).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08399520B2
Quelldatensatzuspto-grants-2013_03
ORD IDord-8fdfb94326544a2c9c87c60ee222323c
Quellennotizuspto-grants-2013_03