HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromo-4-fluoro-2-nitrobenzene → HCID 23087411, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromo-4-fluoro-2-nitrobenzene | HCID 2773383 | — |
| Edukt | 6-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate | HCID 15330256 | — |
| Edukt | Tributyl(4-fluoro-2-nitrophenyl)tin | HCID 23087155 | — |
| Produkt | HCID 23087411 | HCID 23087411 | — |
Reaktionsschritte
Synthesized from 1-bromo-4-fluoro-2-nitrobenzene according to an analogous synthetic method to Preparation Example 76, tributyl(4-fluoro-2-nitrophenyl)tin (7.1 g) and 6-methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate (2.2 g) were used according to an analogous synthetic method to Preparation Example 77 to provide 3-(4-fluoro-2-nitrophenyl)-7-methoxy-1,2-dihydronaphthalene (1.4 g). The total amount of this compound was used according to an analogous synthetic method to Example 30 to provide the title compound (1.1 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08399520B2 |
| Quelldatensatz | uspto-grants-2013_03 |
| ORD ID | ord-8fdfb94326544a2c9c87c60ee222323c |
| Quellennotiz | uspto-grants-2013_03 |