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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1950100Generated: October 30, 2026

4-Bromo-3-nitroanisole → HCID 23087551, compound

https://huagongshe.com/reaction/1950100

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Bromo-3-nitroanisoleHCID 79288—
Reactant(6-Methoxy-1-benzothiophen-2-yl)boronic acidHCID 10560276—
Reactant6-Methoxy-1-benzothiopheneHCID 13634237—
ProductHCID 23087551HCID 23087551—

Reaction Steps

Synthesized from 6-methoxybenzo[b]thiophene according to an analogous synthetic method to Preparation Example 78, (6-methoxybenzo[b]thiophen-2-yl)boronic acid (3.2 g) and 4-bromo-3-nitroanisole (3.4 g) were used according to an analogous synthetic method to Preparation Example 79 to provide 6-methoxy-2-(4-methoxy-2-nitrophenyl)benzo[b]thiophene (1.7 g). Synthesized from this compound (1.9 g) according to an analogous synthetic method to Example 22, the title compound (1.6 g) was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08399520B2
Source datasetuspto-grants-2013_03
ORD IDord-f894c3f634f04e3592142f26d07979b6
Source noteuspto-grants-2013_03