HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-3-nitroanisole → HCID 23087551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-3-nitroanisole | HCID 79288 | — |
| Reactant | (6-Methoxy-1-benzothiophen-2-yl)boronic acid | HCID 10560276 | — |
| Reactant | 6-Methoxy-1-benzothiophene | HCID 13634237 | — |
| Product | HCID 23087551 | HCID 23087551 | — |
Reaction Steps
Synthesized from 6-methoxybenzo[b]thiophene according to an analogous synthetic method to Preparation Example 78, (6-methoxybenzo[b]thiophen-2-yl)boronic acid (3.2 g) and 4-bromo-3-nitroanisole (3.4 g) were used according to an analogous synthetic method to Preparation Example 79 to provide 6-methoxy-2-(4-methoxy-2-nitrophenyl)benzo[b]thiophene (1.7 g). Synthesized from this compound (1.9 g) according to an analogous synthetic method to Example 22, the title compound (1.6 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399520B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-f894c3f634f04e3592142f26d07979b6 |
| Source note | uspto-grants-2013_03 |