HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyloxyacetyl chloride → HCID 57934029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyloxyacetyl chloride | HCID 177085 | — |
| Reactant | HCID 57933922 | HCID 57933922 | — |
| Product | HCID 57934029 | HCID 57934029 | 94.7% |
Reaction Steps
Synthesized from [4-(2-azepan-1-ylethoxy)benzyl]{5-(tert-butyldimethylsilyloxy)-2-[6-(tert-butyldimethylsilyloxy)-1,2,3,4-tetrahydronaphthalen-2-yl]phenyl}amine (400 mg) and benzyloxyacetyl chloride (520 mg) according to an analogous synthetic method to Example 152, the title compound (450 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399520B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-8a56b9d479e24910981009896909e540 |
| Source note | uspto-grants-2013_03 |