HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivalic acid 6-(2-ethylamino-4,5-dimethoxyphenyl)-5,6,7,8-tetrahydronaphthalen-2-yl ester → HCID 9937238, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivalic acid 6-(2-ethylamino-4,5-dimethoxyphenyl)-5,6,7,8-tetrahydronaphthalen-2-yl ester | HCID 57933854 | — |
| Reactant | 5-(2-Azepan-1-ylethyl)pyridine-2-carbonyl chloride hydrochloride | HCID 86605243 | — |
| Product | HCID 9937238 | HCID 9937238 | 18.9% |
Reaction Steps
Synthesized from pivalic acid 6-(2-ethylamino-4,5-dimethoxyphenyl)-5,6,7,8-tetrahydronaphthalen-2-yl ester (40 mg) and 5-(2-azepan-1-ylethyl)pyridine-2-carbonyl chloride hydrochloride (320 mg) according to an analogous synthetic method to Example 152, the title compound (10 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399520B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-1b69ed073e2c4570bdf14dd1a02abeb5 |
| Source note | uspto-grants-2013_03 |