HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxyphthalic acid → 5-Hydroxy-2-{5-methoxy-2-[2-(4-methoxyphenyl)ethyl]phenyl} isoindole-1,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxyphthalic acid | HCID 11881 | — |
| Reactant | 5-Methoxy-2-[2-(4-methoxyphenyl)ethyl]phenylamine | HCID 11219085 | — |
| Product | 5-Hydroxy-2-{5-methoxy-2-[2-(4-methoxyphenyl)ethyl]phenyl} isoindole-1,3-dione | HCID 23087065 | 110.6% |
Reaction Steps
Synthesized from 5-methoxy-2-[2-(4-methoxyphenyl)ethyl]phenylamine (1.5 g) and 4-hydroxyphthalic acid (1.6 g) according to an analogous synthetic method to Preparation Example 112, the title compound (2.6 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399520B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-da4585d9e5d44498a1a7bfb356ca66e8 |
| Source note | uspto-grants-2013_03 |