HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-chloro-N-(1-methylethyl)acetamide → HCID 58023104, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-chloro-N-(1-methylethyl)acetamide | HCID 76171 | — |
| Reactant | Pivalic acid 6-{2-[ethyl(4-hydroxybenzoyl)amino]-4-methoxyphenyl}-5,6,7,8-tetrahydronaphthalen-2-yl ester | HCID 57934562 | — |
| Product | HCID 58023104 | HCID 58023104 | 11.1% |
Reaction Steps
Synthesized from pivalic acid 6-{2-[ethyl(4-hydroxybenzoyl)amino]-4-methoxyphenyl}-5,6,7,8-tetrahydronaphthalen-2-yl ester (25 mg) and 2-chloro-N-isopropylacetamide (13 mg) according to an analogous synthetic method to Example 567 and purified by LC-MS, the title compound (2.7 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399520B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-fd9b35f33cee40b4a3c10971b8e78f8b |
| Source note | uspto-grants-2013_03 |