HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-chloro-N-(2-methoxyethyl)-N-methylacetamide → HCID 57934089, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-chloro-N-(2-methoxyethyl)-N-methylacetamide | HCID 15174913 | — |
| Reactant | pivalic acid (S)-6-{2-[ethyl(4-hydroxybenzoyl)amino]-4-methoxyphenyl}-5,6,7,8-tetrahydronaphthalen-2-yl ester | HCID 57934155 | — |
| Product | HCID 57934089 | HCID 57934089 | 36.3% |
Reaction Steps
Synthesized from pivalic acid (S)-6-{2-[ethyl(4-hydroxybenzoyl)amino]-4-methoxyphenyl}-5,6,7,8-tetrahydronaphthalen-2-yl ester (20 mg) and 2-chloro-N-(2-methoxyethyl)-N-methylacetamide (13 mg) according to an analogous synthetic method to Example 404 and purified by LC-MS, the title compound (7.5 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399520B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-16edacc1e2ef4ba59fa5e5ab0d885f94 |
| Source note | uspto-grants-2013_03 |