HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloro-N,N-diethylacetamide → HCID 66627197, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloro-N,N-diethylacetamide | HCID 16844 | — |
| Reactant | HCID 86605259 | HCID 86605259 | — |
| Product | HCID 66627197 | HCID 66627197 | 47.4% |
Reaction Steps
Synthesized from pivalic acid (R)-6-{2-[(3-fluoro-4-hydroxybenzoyl)methylamino]-4-methoxyphenyl}-5,6,7,8-tetrahydronaphthalen-2-yl ester (20 mg) and 2-chloro-N,N-diethylacetamide (12 mg) according to an analogous synthetic method to Example 404 and purified by LC-MS, the title compound (9.5 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399520B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-ffaa3e36e87a45d9bed273c03a124e88 |
| Source note | uspto-grants-2013_03 |