HuagongsheHuagongshe Chemistry Print Report · For research reference only
Resorcinol → 4,4'-Dimethoxy-2-hydroxybenzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Resorcinol | HCID 5054 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | (2,4-Dihydroxyphenyl)(4-methoxyphenyl)methanone | HCID 350227 | — |
| Product | 4,4'-Dimethoxy-2-hydroxybenzophenone | HCID 96154 | — |
Reaction Steps
Synthesized from resorcinol and 4-methoxybenzoyl chloride according to an analogous synthetic method to Preparation Example 66, (2,4-dihydroxyphenyl)(4-methoxyphenyl)methanone (9.7 g) and methyl iodide (13.1 g) were used according to an analogous synthetic method to Example 383 to provide the title compound (7.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399520B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-9ef8f92995af41c99a14b362515ff8dd |
| Source note | uspto-grants-2013_03 |