HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylic Acid → HCID 140546753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylic Acid | HCID 338 | — |
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | Calcium Hydroxide | HCID 6093208 | — |
| Reactant | HCID 68552206 | HCID 68552206 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 140546753 | HCID 140546753 | — |
Reaction Steps
The title compound in 4 g of base oil XOMAPE 150 (9.12 g, Basicity Index 1.21) was prepared as outlined in Example 4 by employing 5-(pentadecy-2-yl)salicylic acid (Example 9, 3.33 g), a commercial lower alkyl (i.e. less than C20) salicylic acid (Infineum M7103, obtainable from Infineum UK Limited, 3.70 g), xylene (203.33 g), calcium hydroxide (1.56 g), and a promoter (methanol:water (97%:3%), 23.37 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404627B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-5b0df5fe51da4701855d0c75ebaaeca5 |
| Source note | uspto-grants-2013_03 |