HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylmorpholine → HCID 86761782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylmorpholine | HCID 7972 | — |
| Reactant | PyBOP | HCID 2724699 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86761782 | HCID 86761782 | — |
Reaction Steps
Fmoc-amino acid (4 equiv), PyBOP (4 equiv), and NMM (4 equiv) were dissolved in DMF (2 ml) and added to the resin. The reaction mixture was shaken at room temperature for 90 min and washed with DMF (5×2 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404647B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-4ee38fbdd8c14e7c8263b16e92cde1da |
| Source note | uspto-grants-2013_03 |