HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-amino-4-methylbenzoate → HCID 16387575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-amino-4-methylbenzoate | HCID 337778 | — |
| Reactant | 5-Bromothiophene-2-carboxylic acid | HCID 349115 | — |
| Product | HCID 16387575 | HCID 16387575 | 88% |
Reaction Steps
Compound a was prepared by coupling 5-bromothiophene-2-carboxylic acid with commercially available methyl 3-amino-4-methylbenzoate using the method described in Example 128 to afford a white solid in 88% yield. HPLC Ret time=3.25 min. LCMS [M+H]+ 355.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404689B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-ded805350ba9498b9f627919f2943d12 |
| Source note | uspto-grants-2013_03 |