HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Bromide → HCID 67361873, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | HCID 85393728 | HCID 85393728 | — |
| Product | HCID 67361873 | HCID 67361873 | — |
Reaction Steps
From 6a (yield: 84%); mp 154-156° C.; IR (KBr) 3276, 2924, 1684, 1252 cm−1; 1H NMR (400 MHz, CDCl3) δ 1.38 (t, 3H, J=7 Hz), 4.38 (q, 2H, J=7 Hz), 7.05 (d, 1H, J=7 Hz), 7.36 (s, 1H), 7.40 (s, 1H), 7.88 (s, 1H), 8.32 (d, 1H, J=7 Hz), 12.53 (brs, 1H); 13C NMR (100 MHz, CDCl3) δ 14.3, 60.4, 101.5, 106.5, 113.5, 113.7, 124.5, 125.6, 130.3, 133.0, 140.7, 160.6; MS m/z 229 (M+, 73), 183 (100), 155 (20), 129 (9). Anal. Calcd for C12H11N3O2: C, 62.87; H, 4.84; N, 18.33. Found: C, 63.11; H, 4.75; N, 18.22.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404707B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-3a8c0cb8d9e7420ca9ff874bc5be6a72 |
| Source note | uspto-grants-2013_03 |