Potassium Bromide → HCID 67361374, compound

Participants

Reaction Steps

From 6f (yield: 87%); mp 207-209° C.; IR (KBr) 3285, 1681, 1248 cm−1; 1H NMR (400 MHz, CDCl3) δ 1.30 (t, 3H, J=7 Hz), 1.34 (d, 6H, J=7 Hz), 3.11 (sept, 1H, J=7 Hz), 4.42 (q, 2H, J=7 Hz), 6.82 (d, 1H, J=7 Hz), 7.17 (s, 1H), 7.56 (s, 1H), 7.73 (d, 1H, J=7 Hz), 11.40 (brs, 1H); 13C NMR (100 MHz, CDCl3) δ 14.2, 22.5, 28.3, 61.0, 101.0, 107.5, 108.1, 114.1, 123.3, 126.2, 133.2, 141.31, 151.4, 161.9; MS m/z 271 (M+, 82), 256 (40), 225 (42), 210 (100), 182 (20). Anal. Calcd for C15H17N3O2: C, 66.40; H, 6.32; N, 15.49. Found: C, 66.68; H, 6.41; N, 15.57.

Provenance & Evidence