Potassium Bromide → HCID 67363242, compound

Participants

Reaction Steps

From 6g (yield: 57%); mp 276-278° C.; IR (KBr) 1711, 1243, 1175 cm−1; 1H NMR (400 MHz, DMSO-d6) δ 1.38 (m, 12H), 4.36 (q, 2H, J=7 Hz), 6.97 (d, 1H, J=7 Hz), 7.36 (s, 1H), 7.56 (s, 1H), 8.21 (d, 1H, J=7 Hz), 12.43 (brs, 1H); 13C NMR (100 MHz, DMSO-d6) δ 14.2, 30.1, 31.8, 60.3, 100.6, 106.6, 107.2, 113.2, 124.2, 125.5, 124.2, 125.5, 133.0, 140.1, 153.2, 160.6; MS m/z 285 (M+, 57), 270 (38), 224 (100), 196 (17). Anal. Calcd for C16H19N3O2: C, 67.35; H, 6.71; N, 14.73. Found: C, 67.20; H, 6.88; N, 14.51.

Provenance & Evidence