Potassium Bromide → HCID 67362783, compound

Participants

Reaction Steps

From 25a (yield: 35%); mp 168° C.; IR (KBr) 3422, 3053, 2917, 2827, 1637, 1521, 1490, 1307, 1027 cm−1; 1H NMR (400 MHz, DMSO-d6) δ 2.30 (s, 3H), 3.80 (s, 3H), 6.93 (d, 1H, J=7.6 Hz), 7.01 (d, 1H, J=2.0 Hz), 7.03 (m, 2H), 7.49 (s, 1H), 7.77 (m, 2H), 8.02 (d, 1H, J=7.2 Hz), 11.83 (s, 1H); 13C NMR (100 MHz, DMSO-d6) δ 14.2, 55.2, 96.8, 100.5, 109.2, 114.2, 114.4, 120.3, 124.6, 126.0, 131.0, 135.8, 139.0, 140.8, 158.5. Anal. Calcd for C17H15N3O: C, 73.63; H, 5.45; N, 15.15. Found: C, 73.89; H, 5.65; N, 15.13.

Provenance & Evidence