2-Chlorobenzoyl chloride → HCID 44548378, compound

HRID 1951593Notes

Reaction equation

HRID 1951593 reaction equation
C1(C2OC=C(C3C=CC(N)=CC=3)N=2)C=CC=CC=1.[Cl:19][C:20]1[CH:45]=[C:44](Cl)[CH:43]=[CH:42][C:21]=1[C:22]([NH:24][C:25]1[CH:30]=[CH:29][C:28]([C:31]2[N:32]=[C:33]([C:36]3[CH:41]=[CH:40][CH:39]=[CH:38][CH:37]=3)[O:34][CH:35]=2)=[CH:27][CH:26]=1)=[O:23].ClC1C=CC=CC=1C(Cl)=O>>[Cl:19][C:20]1[CH:45]=[CH:44][CH:43]=[CH:42][C:21]=1[C:22]([NH:24][C:25]1[CH:26]=[CH:27][C:28]([C:31]2[N:32]=[C:33]([C:36]3[CH:41]=[CH:40][CH:39]=[CH:38][CH:37]=3)[O:34][CH:35]=2)=[CH:29][CH:30]=1)=[O:23]

Participants

4

Reactant 3

HCID 691102-Chlorobenzoyl chlorideHCID 44548377HCID 44548377, compoundHCID 57465379HCID 57465379, compound

Product 1

HCID 44548378HCID 44548378, compound

Procedure

compound 36 was prepared from 35b in a similar fashion to compound 35 following Method F, except that 2-chlorobenzoyl chloride was used in place of 2,4-dichlorobenzoyl chloride. ESI+ m/z=375.1 [MH]+.

Sources & evidence

ORD record
ord-798968ab27514a69a545ec89806aebfe
Source dataset
uspto-grants-2013_03
Patent number
US08404722B2

Reaction notes

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