Pyrrolidine → HCID 57475112, compound

Participants

Reaction Conditions

Reaction Steps

Pyrrolidine (1.95 g, 2.29 ml, 27.5 mmol), 1,2,3-triazole (2.07 g, 30 mmol) and 4 Å molecular sieve (7.14 g) were added to a solution of 1,4-dioxaspiro[4,5]decan-8-one (3.9 g, 25 mmol) in toluene (40 ml). The mixture was stirred for 7 h at 90° C. Then the solution was decanted and immediately reacted further.

Provenance & Evidence