HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 178439725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | HCID 68600119 | HCID 68600119 | — |
| Product | HCID 178439725 | HCID 178439725 | — |
Reaction Steps
The thus-obtained 3-Allyloxy-5,6,7,8-tetrahydro-1,4-phenanthrenequinone was dissolved in 50 ml of toluene and refluxed for 5 hours and then was concentrated by distillation under reduced pressure and was then purified by chromatography on silica gel to give 7.3 g (27.2 mM) of 2-Allyl-3-hydroxy-5,6,7,8-tetrahydro-1,4-phenanthrenequinone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404869B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-72e08cb5931e419fa0497af3721070aa |
| Source note | uspto-grants-2013_03 |