HCID 86664854, compound → HCID 86664853, compound

Participants

Reaction Steps

The compound 6 (4 mg) obtained above was subsequently reduced by passing H2 through a stirred suspension in EtOAc (2 mL) and 10% Pd—C (4 mg) for 6 hours (or until the reaction completed by NMR). The catalyst was filtered off (Celite), the filtrate was evaporated in vacuo to give 4 mg of the title compound as a crude mixture; 1H NMR (400 MHz, CDCl3) δ 7.82 (m, 4H), 7.70 (m, 4H), 7.20-7.32 (m, 14H), 6.10 (s, 1H), 5.10 (s, 2H), 4.56 (s, 2H), 4.04 (m, 2H), 3.64 (m 4H), 3.25 (m, 4H), 2.09-2.62 (m, 8H), and 1.17-1.62 (m, 23H).

Provenance & Evidence