Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Octadecylamine | HCID 15793 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 85765042 | HCID 85765042 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 53706613 | HCID 53706613 | — |
Reaction Steps
A mixture of 2-ethylhexyl vinylphosphonate (49.90 g), octadecylamine (40.43 g) and sodium hydride 0.10 g was stirred at 140° C. for 6 hours. Water (100 ml) and ethyl acetate (200 ml) were added. The organic phase was separated, dried with sodium sulfate, filtered and the solvent evaporated under reduced pressure to give di(2-ethylhexyl)[2-(octadecylamino)ethyl]phosphonate, as colourless liquid nD40 =1.4541.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06114340 |
|---|
| Source dataset | uspto-grants-2000_09 |
|---|
| ORD ID | ord-3d7be589849a485e92414f071f5f1719 |
|---|
| Source note | uspto-grants-2000_09 |
|---|
