HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalic Anhydride → 1H-Isoindole-1,3(2H)-dione, 2-octadecyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Reactant | Octadecylamine | HCID 15793 | — |
| Product | 1H-Isoindole-1,3(2H)-dione, 2-octadecyl- | HCID 3495344 | 89% |
Reaction Steps
Phthalic anhydride (1.00 g) and octadecylamine (1.82 g) were stirred for 1 hour at 110° C. The reaction mixture was purified by silica gel column chromatography (silica gel 34 g, chloroform:methanol=20:1), thereby yielding 2.40 g of the aimed compound as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114325 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-21eb041e01064c3c8bfaeab295eb43cc |
| Source note | uspto-grants-2000_09 |