HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenepropanal → HCID 70303799, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenepropanal | HCID 7707 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | L-Serine, methyl ester, hydrochloride (1:1) | HCID 2723730 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Palladium | HCID 23938 | — |
| Solvent | HCID 178418361 | HCID 178418361 | — |
| Product | HCID 70303799 | HCID 70303799 | — |
Reaction Steps
L-Serine methyl ester hydrochloride (0.9 moles, 14 g), triethylamine (0.9 moles, 9.1 g) and 3-phenylpropionaldehyde (0.9 moles, 12.1 g) are dissolved in dry methanol (370 ml) in a Parr bottle and hydrogenated under 45 psi in the presence of 10% Pd/C, until the hydrogen absorption ceases.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114391 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-594f2c493cf948a1b4e74d831e303ab0 |
| Source note | uspto-grants-2000_09 |