HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178468113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 137182954 | HCID 137182954 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 178468113 | HCID 178468113 | 63% |
Reaction Steps
Prepared analogously to Example 4c) from (R)-N5 -(amino(nitroimino)-methyl]-N-[[4-[[[bis-(methoxycarbonylmethyl)amino]carbonyl]methyl]phenyl]methyl]-N2 -(diphenylacetyl)-ornithinamide by catalytic hydrogenation in the presence of palladium black and 80% aqueous acetic acid in a yield of 63% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114390 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-d6e3b6914b93467b8e9d93158a5afb4a |
| Source note | uspto-grants-2000_09 |