HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178468095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 178439950 | HCID 178439950 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 178468095 | HCID 178468095 | 54% |
Reaction Steps
Prepared analogously to Example 4c) from (R)-N-[[4-(aminocarbonylaminomethyl)phenyl]methyl]-N5 -[amino(nitroimino)methyl]-N2 -[(7-methyl-2-propyl-1H-benzimidazol-5-yl)carbonyl]-ornithinamide by catalytic hydrogenation in the presence of palladium black and 80% aqueous acetic acid in a yield of 54% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114390 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-1b2b5fd394d941678f29bc47a50e36bf |
| Source note | uspto-grants-2000_09 |