HCID 17910259, compound → HCID 17910223, compound

HRID 1953270Notes

Reaction equation

HRID 1953270 reaction equation
[CH3:1][NH:2][C:3]1[CH:21]=[CH:20][C:6]([C:7]([C:9]2([CH2:15][C:16]([O:18][CH3:19])=[O:17])[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]2)=[O:8])=[CH:5][C:4]=1[N+:22]([O-])=O>CO.[Pd].[H][H]>[CH3:1][NH:2][C:3]1[CH:21]=[CH:20][C:6]([C:7]([C:9]2([CH2:15][C:16]([O:18][CH3:19])=[O:17])[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]2)=[O:8])=[CH:5][C:4]=1[NH2:22]

Participants

4

Reactant 1

HCID 17910259HCID 17910259, compound

Product 1

HCID 17910223HCID 17910223, compound

Reagents, catalysts & solvents 2

HCID 178506449HCID 178506449, compoundCatalystHCID 887MethanolSolvent

Procedure

Prepared analogously to Example 1c from methyl [1-(4-methylamino-3-nitro-benzoyl)-cyclohexyl]-acetate and palladium on activated charcoal/hydrogen in methanol.

Sources & evidence

ORD record
ord-27467b25467f443ba7b12b8ae4f1013a
Source dataset
uspto-grants-2000_09
Patent number
US06114532

Reaction notes

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