HCID 54368038, compound → HCID 54560032, compound

HRID 1953275Notes

Reaction equation

HRID 1953275 reaction equation
[CH2:1]([O:3][P:4]([C:11]1[CH:16]=[CH:15][C:14]([NH:17][CH3:18])=[C:13]([N+:19]([O-])=O)[CH:12]=1)([CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])=[O:5])[CH3:2]>C(O)C.[Pd].[H][H]>[CH2:1]([O:3][P:4]([C:11]1[CH:16]=[CH:15][C:14]([NH:17][CH3:18])=[C:13]([NH2:19])[CH:12]=1)([CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])=[O:5])[CH3:2]

Participants

4

Reactant 1

HCID 54368038HCID 54368038, compound

Product 1

HCID 54560032HCID 54560032, compound

Reagents, catalysts & solvents 2

HCID 178506449HCID 178506449, compoundCatalystHCID 702EthanolSolvent

Procedure

Prepared analogously to Example 1c from ethyl(4-methylamino-3-nitro-phenyl)-n-pentyl-phosphinate and palladium on activated charcoal/hydrogen in ethanol.

Sources & evidence

ORD record
ord-e90e2bd90101439f9fd6b3a50debfd2e
Source dataset
uspto-grants-2000_09
Patent number
US06114532

Reaction notes

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