HCID 54077658, compound → N1-Methyl-4-(phenylsulfonyl)-1,2-benzenediamine

HRID 1953281Notes

Reaction equation

HRID 1953281 reaction equation
[C:1]1([S:7]([C:10]2[CH:15]=[CH:14][C:13]([NH:16][CH3:17])=[C:12]([N+:18]([O-])=O)[CH:11]=2)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>C(Cl)Cl.CO.[Pd].[H][H]>[C:1]1([S:7]([C:10]2[CH:15]=[CH:14][C:13]([NH:16][CH3:17])=[C:12]([NH2:18])[CH:11]=2)(=[O:9])=[O:8])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 1

HCID 54077658HCID 54077658, compound

Product 1

HCID 53887061N1-Methyl-4-(phenylsulfonyl)-1,2-benzenediamine

Reagents, catalysts & solvents 2

HCID 178506449HCID 178506449, compoundCatalystHCID 21226129Dichloromethane methanolSolvent

Procedure

Prepared analogously to Example 1c from (4-benzenesulphonyl-2-nitro-phenyl)-methyl-amine and palladium on activated charcoal/hydrogen in methylene chloride/methanol.

Sources & evidence

ORD record
ord-3d18d9c49ab5462fa692c86aca8d0583
Source dataset
uspto-grants-2000_09
Patent number
US06114532

Reaction notes

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